Sintering of synthesized sialon powders.

Sintering of Zircon Powders

The Effect of Precursor Composition and Sintering Additives on the Formation of β-Sialon from Al, Si and Al2O3 Powders

A study was performed to investigate the effect of increasing the Al or Al2O3 precursor content, above the stoichiometric amount, on the formation of β-sialon by pressureless sintering of Al, Si and Al2O3 powders in flowing nitrogen gas. The effect of adding Y2O3 or Fe to the precursor mixture, on the β-sialon formation, was also studied. The phase morphology and yield produced by the various c...

Oxidation of Ca-α-SiAlON Powders Prepared by Combustion Synthesis

The oxidation of Ca-α-SiAlON synthesized by the combustion synthesis (CS) method with different additives was investigated in air atmosphere using thermogravimetric (TG) analysis in a temperature range from 1453 K to 1653 K. The experimental results indicated that oxidation was controlled by mixed chemical and diffusion steps. The oxidation products by XRD analysis were composed of SiO₂ and CaA...

Sintering of Fine Oxide Powders: II, Sintering Mechanisms

Conventional and new sintering mechanisms have been porous compacts is well-known in the ceramic literature. However, several reports have been presented recently that investigated using fine powders of CeO2 and Y2O3 of excellent sinterability. We have verified the validity of Herring’s show that particle/grain size can remain essentially constant up to a density of 92%, and such a resistance t...

Full densification of Molybdenum powders using Spark Plasma Sintering

Pure molybdenum powder was sintered using Spark Plasma Sintering under various temperatures, and holding times, under a pressure of 77 MPa and a heating rate at 700°C/min. After sintering, a carbide layer was observed at the surface. The carbide layer thickness, the relative density of the sample as well as the microhardness and the grain size of Mo were measured. The carbide thickness depends ...